External Parameter

Contents

Introduction

Project with External Parameter

Data Source

Kinetic Model

Simulation: Predictions and Optimization

How To Guide

 

Introduction

Dependence on external parameter is implemented in Kinetics Neo since version 3.0.

The rate of chemical reactions and crystallization depends on different parameters, the first of them is temperature.

Now we have the possibility to use the second parameter in the common kinetic model, where reaction rate depends on two parameters. In the software it is called External Parameter.

Examples of the External Parameter:

  • Partial pressure of reactive gaseous component in the surrounding atmosphere, like oxidation reactions.

 

Project with External Parameter

Using of External Parameter in the kinetic project must be set in the Project properties in Settings (File - Project):

 

Data Source

For each data file in the Source Data the value of the external parameter must be set during Data Preparation:

Please use bar units for pressure, and relative units for other external parameters, where data with value 1 for External Parameter must be present.

 

Kinetic Model

Only Model-Based analysis can be used to create the kinetic model depending on temperature and external parameter (like pressure).

Model-Free analysis is not suitable for kinetic analysis of such data in Kinetics Neo.

If the project uses External Parameter, then each reaction step in the kinetic model contains the checkbox to set if this step depends on this External Parameter or not. If selected parameter for the project is Pressure, then the checkbox Depends on: Pressure is shown.

In multi-step models the dependence on the External Parameter can be set for each reaction step separately. For example, some reactions steps in the model are pressure-dependent, and other steps - not.

Each reaction step, depending on the External Parameter, contains additional parameter for this dependence. For example, for pressure-dependent reactions the name of additional parameter is nPressure. The value of this parameter can be different for different reaction steps in the kinetic model.

 

Simulation: Predictions and Optimization

If the project uses External Parameter, then the Simulation (both Prediction and Optimization) can be done for given value of external parameter.

The next Dynamic Prediction is done for pressure-dependent reaction for different heating rates at pressure 0.5 bar.

 

How To Guide

The example of kinetic model for pressure-dependent reaction can be found on our web site in our guide How to Analyze Reversible Reaction with Reactive Gaseous Reactant.